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PAT for pharmaceutical manufacturing process involving solid dosages forms

By Román-Ospino, Andrés D; Cárdenas, Vanessa Ortega-Zuñiga, Carlos; Singh, Ravendra

Published on

Abstract

This chapter summarizes important considerations to develop multivariate methods for pharmaceuticals process monitoring and quality control in solid dosages forms based on spectroscopic techniques. The stages described in each section aimed to explain relevant knowledge of the calibration procedure, model development, and estimation of sampling error. Basic principles of near-infrared spectroscopy and the interaction between organic particles and light correspond to a critical step toward the construction of robust spectroscopic methods. The understanding of this process will allow the extraction of useful information for the calibration purpose highlighting the quality attribute of interest in the spectroscopic signal. The chapter aims to provide basic knowledge for xperts who want to apply NIR spectroscopy in combination with multivariate analysis as PAT tools for quality control.

Journal

Computer Aided Chemical Engineering. Volume 41, 2018, 293-315

DOI

10.1016/B978-0-444-63963-9.00012-9

Type of publication

Peer-reviewed journal

Affiliations

  • Rutgers, The State University of New Jersey

Article Classification

Research Article

Classification Areas

  • Oral doses
  • Modeling

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