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1. Solvothermal Crystallization Kinetics and Control of Crystal Size Distribution of MOF-808 in a Continuous Flow Reactor

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   09 Jun 2023 | Contributor(s):: Bagi, Sujay D., Myerson, Allan S. Román-Leshkov, Yuriy, Román-Leshkov, Yuriy

   A fundamental understanding of the crystallization pathways for metal-organic frameworks (MOFs) allows for exploring the untapped combinatorial space of the organic and inorganic building units, creating possibilities to synthesize highly crystalline frameworks with desired physicochemical...

2. Evaluation of crystallization kinetics of adipic acid in an oscillatory baffled crystallizer

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   09 Jun 2023 | Contributor(s):: Brown, C. J., Ni, X.

   For solution crystallization, nucleation can be characterized by the maximum sub-cooling (or metastable limit), which is known to vary with numerous process parameters. The relationship between the metastable limit and cooling rate is of particular interest, as it can be utilized to derive...

3. Design and optimization of a multistage continuous cooling mixed suspension, mixed product removal crystallizer

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   09 Jun 2023 | Contributor(s):: Power, Graham, Hou, Guangyang Kamaraju, Vamsi Krishna Morris, Gary, Zhao, Yan, Glennon, Brian

   Continuously operated single and multistage MSMPR crystallizers using intermittent withdrawal through use of an automated pressure supply were developed for the cooling crystallization of Paracetamol from an aqueous isopropanol mixture. The onset of steady state was detected through analysis of...